Technical Note

      Abstract    

        

STANDARD OPERATING PROCEDURE (SOP) FOR MICROWAVE DIGESTION SYSTEM (MDS-10)

 A.K. Jaiswal, Anita Yadav, T.Millo, S.K Gupta

 

ABSTRACT: Microwave digestion system plays very important role for digestion on different samples such as tissues,blood,hair,nails,rocks,minerals etc during sample preparation for analytical purposes. Its use is readily understood from breadth of its applications. The range of material that can be analyzed by Microwave digestion system is essentially unlimited. Applications are found in diverse fields such as forensic science, pharmaceuticals, food and agriculture, biological and clinical chemistry, environmental chemistry and many others. Standard operating procedure for Sineo make&model MDS10 Microwave digestion system have been developed. The different steps involved for smooth running of microwave digestion system has been successfully explained.

KEY WORDS: Standard operating procedure(SOP),microwave digestion, MDS-10, blood, tissue, urine, etc.

REFERENCES:

 

  1. Jaiswal AK, Kaushal P, Dhar P, Millo T and Murthy OP. Microwave digestor and its forensic application- a review. Journal of Forensic Medicine & Toxicology 28(1):65-74.

  2. .H.M. Kingston, P.J. Walter, “The Art and Science of Microwave Sample Preparations for Trace and Ultratrace Elemental Analysis” In Inductively Coupled Mass Spectrometry, A. Montaser, Wiley-VCH, 1997.

  3. Bloom, N.S.; Miklavcic, V.L.; Prestbo, E.M. "Determination of Mercury in Fossil Fuels at the ppb Level by Cold Vapor Atomic Fluorescence Spectrometry, after Total Wet Oxidation with krchloric Acid in Teflon Micmwdve Digestion Bombs." Resented at the Conference on Managing Air Toxics: State ofthe Art. Washington, DC. July 13-1S, 1993.

  4. Razuin R, Rohayu SA, Mahmood MS, Krishnan RI, Patricia Ann C, Samberkar PN. “Fatal Head Injury in Motor Vehicle Accidents: A Descriptive Study of 37 Autopsies.” JOURNAL OF FORENSIC MEDICINE & TOXICOLOGY, ISSN 0971-1929, Volume 28, No. 1, Jan - June. 2011, 39-45

  5. Matusiewiu, H.; Sturgeon, R.E.; Berman, S.S. 'Trace Element Analysis of Biological Material Following Pressure Digestion with Nitric Acid-Hydrogen Rroxide and Microwave Heating," Journal of AM & tiCd Atomic Speammetry 1989, 4.

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